真空感应悬浮熔炼技术制备高温钛合金及其力学性能演变规律
CSTR:
作者:
作者单位:

攀枝花学院 钒钛学院, 四川 攀枝花 617000

作者简介:

于玉城(1973—),男,黑龙江海林人,博士,副教授,主要从事钛合金及表面技术相关研究工作。

通讯作者:

中图分类号:

TF823;TF125.2+2

基金项目:

“材料腐蚀与防护四川省重点实验室”开放课题基金项目(2022CL13)


Preparation of high temperature titanium alloy by vacuum induced suspension melting and its mechanical properties evolution
Author:
Affiliation:

College of Vanadium and Titanium, Panzhihua University, Panzhihua 617000 , China

Fund Project:

  • 摘要
  • |
  • 图/表
  • |
  • 访问统计
  • |
  • 参考文献
  • |
  • 相似文献
  • |
  • 引证文献
  • |
  • 资源附件
  • |
  • 文章评论
    摘要:

    本研究采用真空感应悬浮熔炼法制备高温钛合金铸锭,合金名义成分为Ti-5.8Al-3Sn-8Zr-0.5Mo-0.7Nb-0.25Si。利用金相显微镜、X射线衍射仪、万能拉伸试验机、热模拟试验机等手段和方法研究厚壁钛合金铸件从芯部到边缘的显微组织和力学性能演变规律。试验结果表明:钛合金铸锭芯部由于冷却速度较慢,形成了α-Ti层片较宽的网篮组织,随测试位置由芯部向边缘移动,α-Ti层片逐步细化,层片宽度由6.65μm减小到2.99μm,值得注意的是处于芯部和边缘之间的α-Ti层片宽度波动幅度较大,分布不均匀。室温拉伸性能表明,芯部到边缘的强度变化呈现先下降后升高的规律,且边缘位置与芯部强度值相近,归因于铸造缺陷对力学性能的恶化效果明显弱化了细晶强化效果。高温拉伸变形机制主要受位错滑移机制和扩散变形机制共同控制,600~700℃温度范围内,温度越高,强度越低延伸率越好,边缘样品的抗拉强度比芯部略高,且随温度增加其强度差有缩减趋势;热压缩性能测试表明,在950℃下,不同取样位置的钛合金极限压缩强度差异不大,芯部位置强度略高于边缘位置,950℃条件下材料的变形机制完全为高温扩散型变形机制。

    Abstract:

    High temperature titanium alloy ingot was prepared by vacuum induction suspension melting in this paper, and the nominal composition of alloy was Ti-5.8Al-3Sn-8Zr-0.5Mo-0.7Nb-0.25Si. Metallographic microscope, X-ray diffractometer, universal tensile testing machine and thermal simulation testing machine were used to research the evolution of microstructure and mechanical properties of large size titanium alloy ingot from the center to the edge. The experimental results show that the basket structure formed with the wider α-Ti lamella due to the slow cooling rate of the center of the titanium alloy ingot. The lamella width of α-Ti gradually reduced from 6.65μm to 2.99μm as the test location moved from the center to the edge, however, it is worth noting that the width of the α-Ti lamella in the middle position between the center and the edge fluctuated greatly and the distribution was uneven. Tensile properties at room temperature show that the strength from the centerto the edge decreases first and then increases, and the edge position has little difference with the strength of the center because the deterioration effect of defects on mechanical properties weakens the strengthening effect of fine-grained strengthening. The mechanism of high-temperature tensile deformation was mainly controlled by dislocation slip mechanism and diffusion deformation mechanism. At temperatures ranging from 600℃ to 700℃, the higher the temperature, the lower the strength and the better the elongation. The tensile strength of the edge sample was slightly higher than that of the center, and there was a trend of reducing the strength difference as the temperature increases. The hot compression test showed that the limiting compressive strength of the titanium alloy at 950℃ was almost the same for different sampling positions, with the strength of the center position slightly higher than that of the edge position. At 950℃, the deformation mechanism of the material wass completely a high-temperature diffusion-type deformation mechanism.

    参考文献
    相似文献
    引证文献
引用本文

于玉城,王振玲,杨绍利,等. 真空感应悬浮熔炼技术制备高温钛合金及其力学性能演变规律[J].中国有色冶金,2025,54(1):15-22.

复制
分享
相关视频

文章指标
  • 点击次数:
  • 下载次数:
  • HTML阅读次数:
  • 引用次数:
历史
  • 收稿日期:2024-09-05
  • 最后修改日期:
  • 录用日期:
  • 在线发布日期: 2025-12-18
  • 出版日期:
文章二维码