Abstract:In view of the problems of less theoretical experiments and insufficient research on process diversification in the treatment of zinc leaching residue by SO2 reduction leaching process, the experimental study on the treatment of high-iron acid leaching residue by pre-acidification and SO2 reduction leaching process was carried out to explore the effect of pre-acidification on the zinc leaching rate of SO2 reduction leaching, the reaction time of SO2 reduction leaching section and the sedimentation of pulp after reduction. The results show that the leaching rate of zinc can reach 96% and the reaction time of SO2 reduction section can be shortened to 1.5h under the conditions of concentrated sulfuric acid concentration of 100g/L, reaction temperature of 90℃ and reaction time of 1.5h. When the concentration of pre-acidified sulfuric acid is 90~110g/L, the slurry sedimentation after reduction is better.